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    Synthesis and Investigating of the Novel of Es-Pani@PdNPs Nanocomposite

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    MIPA_JURNAL_Synthesis and Investigating of the Novel of Es-Pani@PdNPs Nanocomposite.pdf (5.398Mb)
    Date
    2023-02
    Author
    BUSRONI, Busroni
    SUYANTA, Suyanta
    ANWAR, Chairil
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    Abstract
    The aim of this research is the synthesize materials Novel of ESPANI@PdNPs nanocomposites obtained chemically. The synthesis of ES-PANI@PdNPs nanocomposite was prepared by the chemical method using FeCl3 as a redox initiator (insitu) and refluxed for 48 hours at 500C, then dried at 500C for 24 hours, obtained a brown-black solid and no water-soluble.The nanocomposite is characterized by UVVis and Fourier transform infrared (FTIR) spectroscopy, the composite shows absorption of Pd(0) nanoparticles along with ES-PANI peaks at 312 nm. FTIR and UV-visible spectra show an interaction between Pd(0) and ES-PANI. This indicated that Pd(0) zero valence had been formed and that internal reduction processes had occurred by imines and amines toward Pd(II) ions.
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    https://repository.unej.ac.id/xmlui/handle/123456789/113285
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    Indonesia DSpace Group :

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