One-Step Synthetic Ofp-Tert-Butylcalix[4]Arene Derivative via Direct Benzoylation: Mechanism Reaction Studies

dc.contributor.author	BUSRONI, Busroni
dc.contributor.author	SANTOSA, Sri Juari
dc.contributor.author	ANWAR, Chairil
dc.date.accessioned	2023-03-16T04:55:48Z
dc.date.available	2023-03-16T04:55:48Z
dc.date.issued	2022-11
dc.identifier.uri	https://repository.unej.ac.id/xmlui/handle/123456789/112950
dc.description.abstract	The aim of research the synthesis of 5,11,17,23-tetra(t-butyl)-25- monohydroxy-26,27,28-tribenzoyloxycalix[4]arene (TBMTCA) material were by one-step synthesized by benzoylation reaction of 5,11,17,23-tetra(t-butyl)-25,26,27,28-tetrahydroxycalix[4]arene (TBCA) and benzoyl chloride is (1: 3,7) mol and the refluxing 3 hours at room temperature and predicted mechanism reaction models. The product reaction of synthesis was carried out by means of FTIR and 1H-NMR spectroscopy. The results material of5,11,17,23-tetra(tbutyl)-25-monohydroxy-26,27,28-tribenzoyloxycalix[4]arene (TBMTCA)synthesized was light yellow crystalline having melting point 306-3090C in 90,2 % yields.	en_US
dc.language.iso	en	en_US
dc.publisher	International Journal of Advanced Research	en_US
dc.subject	TBCA	en_US
dc.subject	TBMTCA	en_US
dc.subject	Benzoylation	en_US
dc.subject	Mechanism Reaction Models	en_US
dc.title	One-Step Synthetic Ofp-Tert-Butylcalix[4]Arene Derivative via Direct Benzoylation: Mechanism Reaction Studies	en_US
dc.type	Article	en_US